Cascade radical synthesis of heteroarenes via iminyl radicals

Journal of the Chemical Society, Perkin Transactions 1 · 2002 · 10.1039/B108323F

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★ 3.0 1 rating
5 : Major extension (new functional group) –
4 : Minor extension (no new functional group) –
3 : Reproduced as published ×1
2 : Reproduced with deviation –
1 : Did not work –
– : Extension failed / Inconclusive –

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PhD student
13 Jul 2026
★ 3 : Reproduced as published

The synthesis from 5a through 6b, to 7b, finally to 8b worked without a problem on 2.0 g scale (in each step).
The yields were comparable to the reported values.