I2-Mediated Diversity Oriented Diastereoselective Synthesis of Amino Acid Derived trans-2,5-Disubstituted Morpholines, Piperazines, and Thiomorpholines

Saurav Bera, Gautam Panda

ACS Combinatorial Science · 2012 · 10.1021/co200129t

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★ 1.0 1 rating
5 : Major extension (new functional group)
4 : Minor extension (no new functional group)
3 : Reproduced as published
2 : Reproduced with deviation
1 : Did not work ×1
: Extension failed / Inconclusive

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PhD student
13 Jul 2026
★ 1 : Did not work

I have tried the iodoetherification as suggested in the paper, with R = H and NBn instead of NTs. Unfortunately I only saw a mixture of unidentified products.